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SEM back online

SEM back online

A couple of months ago, Milly started having beam issues. At the time it seemed like emitter trouble. New emitter modules run about $3k, so I took the opportunity to look into manufacturing …
2015-11-30
microscopy
#Milly #SEM
Cheap digital optical microscope

Cheap digital optical microscope

I recently picked up an AmScope SE400Z inspection scope. It’s a handy desktop microscope that sells for under $200. The large area under the objective lens leaves plenty of room to work, and the 10-20…
2015-11-11
microscopy

Etching tungsten

Electroetching a recrystallized tungsten wire in 2.5 molar sodium hydroxide solution. The cathode is a hunk of highly ordered pyrolytic graphite. I’m doing a couple of test etches. If all goes well, o…
2015-10-11
chemistry
Who needs overhead lights?

Who needs overhead lights?

…when you’ve got tungsten to recrystalize?
2015-10-10
electricity > microscopy

Time for science!

Today’s experiment: tungsten wire recrystallization.
2015-10-03
materials
Puss in Boots

Puss in Boots

[Crouching tiger, hidden Walken. Hypnotic, isn't it? If you’ve never seen Christopher Walken in Puss in Boots, add it to your queue right now. That’s him as Puss, craftily stalking a bird for supper. …
2015-08-30
hackery
All that glitters…

All that glitters…

[Gold particles on carbon at x50,000 Here’s an image of a gold calibration target. To give you an idea of the scale, that line representing 100 nanometers is roughly the diameter of the HIV virus…
2015-06-16
microscopy
Megapixel images from an analog SEM

Megapixel images from an analog SEM

I recently posted my first batch of photos from Milly. While I am happy with her beam performance, I was dissatisfied with the digital photo quality. Until now: It's amazing what a difference a cheap&…
2015-06-02
microscopy
#Milly #SEM
Big SEM: online

Big SEM: online

I recently got Milly the big SEM online. She had a ton off issues that I’ll chronicle in future posts. But rather than dwell on her past, let’s see what she can do. Remember that 2mm stainless sc…
2015-05-31
microscopy
#Milly #SEM

Laser HV repair

I’m in the process of upgrading the brain in the laser from a cheap (and recently deceased) Chinese special to a new design based on the open source Lasersaur. More on that later. I was right in the m…
2015-04-04
electricity > lasers
#don't look at laser with remaining eye
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